NCT05650840

Brief Summary

The aim of the study is to clinically evaluate the efficacy of external stain removal of an activated charcoal based tooth paste versus calcium carbonate /perlite tooth paste. Additionally, to investigate enamel surface abrasion for both toothpastes in vitro.

Trial Health

35
At Risk

Trial Health Score

Automated assessment based on enrollment pace, timeline, and geographic reach

Trial has exceeded expected completion date
Enrollment
38

participants targeted

Target at P25-P50 for not_applicable

Timeline
Completed

Started Jan 2023

Shorter than P25 for not_applicable

Status
unknown

Health score is calculated from publicly available data and should be used for screening purposes only.

Trial Relationships

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Study Timeline

Key milestones and dates

First Submitted

Initial submission to the registry

November 24, 2022

Completed
20 days until next milestone

First Posted

Study publicly available on registry

December 14, 2022

Completed
18 days until next milestone

Study Start

First participant enrolled

January 1, 2023

Completed
5 months until next milestone

Primary Completion

Last participant's last visit for primary outcome

June 1, 2023

Completed
2 months until next milestone

Study Completion

Last participant's last visit for all outcomes

August 1, 2023

Completed
Last Updated

December 28, 2022

Status Verified

December 1, 2022

Enrollment Period

5 months

First QC Date

November 24, 2022

Last Update Submit

December 24, 2022

Conditions

Keywords

Charcoal based toothpasteExternal tooth stainsTeeth abrasion

Outcome Measures

Primary Outcomes (2)

  • Stain scores as per Macpherson modification of the Lobene stain index

    Stain scores will be recorded as per the Macpherson modified Lobene Stain Index area x intensity (AXI). Each tooth will be divided into four areas for assessment: gingival, mesial, distal and body. The stain index will measure area and intensity of extrinsic tooth stain on the facial surfaces of the anterior teeth. The criteria and codes for intensity were: 0: no stain present, natural tooth colouration 1. faint stain 2. clearly visible stain, orange to brown (moderate stain) 3. dark stain, deep brown to black (heavy stain) The area (extent) of the stain was recorded only if an intensity score was of 2 or 3 The area criteria and codes for approximal and gingival sites were: 1. thin line, can be continuous (\< 1/3) 2. thick line or band (\>1/3, \<2/3) 3. covering total area (\> 2/3)

    Baseline

  • Stain scores as per Macpherson modification of the Lobene stain index

    Stain scores will be recorded as per the Macpherson modified Lobene Stain Index area x intensity (AXI). Each tooth will be divided into four areas for assessment: gingival, mesial, distal and body. The stain index will measure area and intensity of extrinsic tooth stain on the facial surfaces of the anterior teeth. The criteria and codes for intensity were: 0: no stain present, natural tooth colouration 1. faint stain 2. clearly visible stain, orange to brown (moderate stain) 3. dark stain, deep brown to black (heavy stain) The area (extent) of the stain was recorded only if an intensity score was of 2 or 3 The area criteria and codes for approximal and gingival sites were: 1. thin line, can be continuous (\< 1/3) 2. thick line or band (\>1/3, \<2/3) 3. covering total area (\> 2/3)

    after four weeks

Other Outcomes (1)

  • enamel abrasion using atomic force microscopy before and after brushing (Anton Paar - Tosca™ 200 - atomic force microscope, USA.)

    3 minutes equivalent to 2 times a day for one month

Study Arms (2)

Charcoal -based whitening toothpaste

EXPERIMENTAL

signal charcoal white\& Detox toothpaste Unilever Mashreq - Egypt

Procedure: Charcoal based whitening toothpaste (signal charcoal white& Detox toothpaste Unilever Mashreq - Egypt

Calcium carbonate /perlite containing whitening toothpaste

ACTIVE COMPARATOR

signal whitening moonlight toothpaste Unilever Mashreq - Egypt

Procedure: Calcium carbonate /perlite containing whitening toothpaste (signal whitening moonlight toothpaste Unilever Mashreq - Egypt).

Interventions

The labial surface of anterior teeth will be brushed by the circular brushing technique twice daily (morning and after 6 hours) for at least 1 minute using charcoal containing toothpaste. Soft bristles toothbrushes will provided to all patients (Oral-B). After 1 month, re-evaluation of the stains will be performed and the data will be recorded. Intervention drug : whitening toothpaste charcoal based whitening toothpaste compared to calcium carbonate and perlite whitening toothpaste FOR IN VITRO: Human premolars will be obtained from volunteers due to orthodontic reasons. Teeth will be divided into two equal groups (n:18) according to the toothpaste used. Teeth will be brushed with an electric tooth brush (Oral-B PRO 500) that will be held in a holder to standardize the position to the tooth surface for 3 minutes equivalent to 2 times a day for one month. Teeth will be prepared for AFM examination

Charcoal -based whitening toothpaste

The labial surface of anterior teeth will be brushed by the circular brushing technique twice daily (morning and after 6hours) for at least 1 minute using calcium carbonate /perlite containing toothpaste. Soft bristles toothbrushes will provided to all patients (Oral-B). After 1 month, re-evaluation of the stains will be performed and the data will be recorded. The main operator will perform the tooth brushing procedures for all the patients himself twice daily. FOR IN VITRO: Human premolars will be obtained from volunteers due to orthodontic reasons. Teeth will be divided into two equal groups (n:18) according to the toothpaste used. Teeth will be brushed with an electric tooth brush(Oral-B PRO 500) that will be held in a holder to standardize the position to the tooth surface for 3 minutes equivalent to 2 times a day for one month. Teeth will be prepared for AFM examination Device used is atomic force microscopy to determine enamel abrasion after brushing

Calcium carbonate /perlite containing whitening toothpaste

Eligibility Criteria

Age18 Years - 50 Years
Sexall
Healthy VolunteersYes
Age GroupsAdult (18-64)

You may qualify if:

  • Adult male and female patients ≥18 years.
  • Good oral and general health and oral hygiene have at least eight natural anterior teeth (incisors and canines) assessable for extrinsic stain and be available for all study appointments.

You may not qualify if:

  • Uncooperative behavior.
  • Patients allergic to tooth paste material.
  • Patient with history of medical disease, drug therapies or any other serious relevant problem.
  • Pregnant or breastfeeding women.
  • Patients with fixed orthodontic appliances
  • Patients who had professional tooth whitening, within the last six months.
  • Patients who had significant amounts of calculus on facial surfaces of the incisors/canines.
  • Patients who had undergone professional periodontal treatment within the previous six months or used mouth rinses for the treatment/ control of a periodontal condition.
  • Patients who had advanced periodontal disease on anterior teeth.
  • Xerostomic patients.
  • Patients who used medications which could affect saliva flow or cause staining.
  • Patients who had undergone dental prophylaxis within 8 weeks of screening.
  • Patients who used minocycline or doxycycline within 30 days of screening or between screening and baseline.
  • ▪ Vital anterior maxillary and mandibular teeth free of caries or restorations, no cervical lesions and no periodontal disease.
  • Intrinsically Discolored teeth caused by tetracycline, fluorosis, hypocalcification hyperplasia, endodontic treatment (or requiring endodontic treatment).
  • +7 more criteria

Contact the study team to confirm eligibility.

Sponsors & Collaborators

MeSH Terms

Conditions

Tooth Abrasion

Interventions

Calcium Carbonate

Condition Hierarchy (Ancestors)

Tooth WearTooth DiseasesStomatognathic Diseases

Intervention Hierarchy (Ancestors)

Calcium CompoundsInorganic ChemicalsCarbonatesCarbonic AcidCarbon Compounds, InorganicMinerals

Study Officials

  • Iman I ElSayad

    Cairo University

    STUDY DIRECTOR
  • Mohamed R El-Bialy, Post Phd

    Cairo University

    STUDY DIRECTOR

Central Study Contacts

Iman I ElSayad, Professor

CONTACT

Mohamed R El-Bialy, Post Phd

CONTACT

Study Design

Study Type
interventional
Phase
not applicable
Allocation
RANDOMIZED
Masking
SINGLE
Who Masked
OUTCOMES ASSESSOR
Purpose
TREATMENT
Intervention Model
PARALLEL
Sponsor Type
OTHER
Responsible Party
PRINCIPAL INVESTIGATOR
PI Title
Master student, conservative department, faculty of dentistry

Study Record Dates

First Submitted

November 24, 2022

First Posted

December 14, 2022

Study Start

January 1, 2023

Primary Completion

June 1, 2023

Study Completion

August 1, 2023

Last Updated

December 28, 2022

Record last verified: 2022-12

Data Sharing

IPD Sharing
Will not share